Synthesis and Characterization of Po

Synthesis and Characterization of Poly(ether amide)s Containing Bisphthalazinone and Ether Linkages

A novel aromatic diacid, 4, 4'-bis[2-(4-carboxyphenyl)phthalazin-1-one-4-yl]-bisphenyl ether Ⅲ, containing bisphthalazinone and ether linkages was prepared from nucleophilic substitution of p-chlorobenzonitrile with the bisphenol-like monomer Ⅰ, followed by alkaline hydrolysis of the intermediate dinitrile Ⅱ. A series of poly(ether amide)s containing bisphthalazinone and ether linkages derived from diacid Ⅲ and aromatic diamines were synthesized by one-step solution condensation polymerization using triphenyl phosphite and pyridine as condensing agents. Moreover, the properties of poly(ether amide)s including thermal stability,solubility and crystallinity were also studied.

作 者： Cheng Liu Shou Hai ZHANG Ming Jing WANG Qi Zhen LIANG Xi Gao JIAN   作者單位： Department of Polymer Science & Materials, Dalian University of Technology, Dalian 116012  刊 名： 中國化學快報（英文版）  ISTIC SCI 英文刊名： CHINESE CHEMICAL LETTERS  年，卷(期)： 2005 16(4)  分類號：   關鍵詞： Poly(ether amide) s   bisphthalazinone   thermal stability   solubility  

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